@article {358, title = {Measurement of dipolar couplings in partially oriented molecules by local field NMR spectroscopy with low-power decoupling}, journal = {Journal of Magnetic Resonance}, volume = {158}, year = {2002}, note = {J Magn Reson619VETimes Cited:8Cited References Count:23}, month = {Sep-Oct}, pages = {52-59}, abstract = {

Low-power phase-modulated Lee-Goldburg homonuclear decoupling was used to record PDLF spectra of fluorine-substituted benzene derivatives dissolved in nematic thermotropic liquid crystalline solvents. The low-power decoupling minimizes sample heating during RE irradiation while still achieving highly resolved PDLF spectra. The method is illustrated by recording spectra for 1,3-dichloro-4-fluoro-5-nitrobenzene, 1,3-dichloro-4-fluorobenzene, and 1, 2-difluoro benzene dissolved in different nematic solvents. (C) 2002 Elsevier Science (USA). All rights reserved.

}, keywords = {resolution}, isbn = {1090-7807}, doi = {Doi 10.1016/S1090-7807(02)00059-9}, url = {://WOS:000179497500006}, author = {Marjanska, M. and Castiglione, F. and Walls, J. D. and Pines, A.} }