|Title||Measurement of dipolar couplings in partially oriented molecules by local field NMR spectroscopy with low-power decoupling|
|Publication Type||Journal Article|
|Year of Publication||2002|
|Authors||Marjanska M., Castiglione F., Walls J.D, Pines A|
|Journal||Journal of Magnetic Resonance|
Low-power phase-modulated Lee-Goldburg homonuclear decoupling was used to record PDLF spectra of fluorine-substituted benzene derivatives dissolved in nematic thermotropic liquid crystalline solvents. The low-power decoupling minimizes sample heating during RE irradiation while still achieving highly resolved PDLF spectra. The method is illustrated by recording spectra for 1,3-dichloro-4-fluoro-5-nitrobenzene, 1,3-dichloro-4-fluorobenzene, and 1, 2-difluoro benzene dissolved in different nematic solvents. (C) 2002 Elsevier Science (USA). All rights reserved.
|URL||<Go to ISI>://WOS:000179497500006|
|Short Title||Measurement of dipolar couplings in partially oriented molecules by local field NMR spectroscopy with low-power decoupling|